##TITLE= NH 171; Ethyl 3-Chloropyrazine-2-carboxylate / CDCl3 APT ##JCAMP-DX= 5.00 $$ Varian Associates, Inc., VNMR Software $$ VNMR Version 5.1 Revision A, March 1, 1995 $$ Tue May 7 08:47:48 MET DST 2002 $$ svsj version 5.1, 97/1/14; hz2ppm (NH) ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= varian ##OWNER= N. Haider, University of Vienna ##SPECTROMETER/DATA SYSTEM= Varian UNITYplus-300 ##.OBSERVE FREQUENCY= 75.4291310 ##.OBSERVE NUCLEUS= ^13C ##.SOLVENT REFERENCE= 77.009 $$ solvent=cdcl3 ##.FIELD= 7.04 $$ Tesla ##.ACQUISITION TIME= 1.8150912 $$ seconds ##.AVERAGES= 128 $$ number of transients ##RESOLUTION= 0.504 $$ digital resolution in Hz ##.PHASE 0= -123.5 $$ zero order phase correction (left edge) ##.PHASE 1= 0.010821 $$ first order phase correction, deg/Hz ##$REFERENCE_POINT= 824.215 $$ Referencing label $$ Varian specific parameters $$ -------------------------- ##$acqstatus= (0..1) 16 16 ##$alfa= 19.9999923706 $$ usec ##$alock= ##$array= <> ##$arraydim= 1 ##$arrayelemts= 0 ##$at= 1.8150912 ##$bs= 16 ##$celem= 0 ##$cp= ##$ct= 128 ##$d1= 2 $$ sec ##$d2= 0.006 $$ sec ##$d3= 0.0010000000475 $$ sec ##$date= ##$dfrq= 299.9479281 $$ Hz ##$dm= ##$dmf= 12000 ##$dmm= ##$dn=

##$dod= 0.00999999977648 $$ sec ##$dof= 0 $$ Hz ##$dp= ##$dpwr= 41 ##$exppath= ##$fb= 9200 ##$file= ##$filter= 0 ##$fn1= 1024 ##$homo= ##$hs= ##$hst= 0.00800000037998 $$ sec ##$il= ##$in= ##$lb1= 0.318309992552 ##$lb= 1 ##$load= ##$loc= 0 ##$math= ##$method= ##$np= 59904 ##$nt= 16384 ##$p1= 28 $$ usec ##$pad= 2 $$ sec ##$parversion= 4.3 ##$pmode= ##$pp= 17.5 $$ usec ##$priority= 5 ##$proc1= ##$proc= ##$pslabel= ##$pw90= 12.9999923706 $$ usec ##$pw= 7 $$ usec ##$rfband= ##$rof1= 10 $$ usec ##$rof2= 9.9999961853 $$ usec ##$seqfil= ##$sfrq= 75.429131 ##$sn= 20 ##$solvent= ##$ss= 0 ##$sw= 16501.650165 ##$temp= 28 ##$tin= ##$tn= ##$tof= 0 $$ Hz ##$tpwr= 53 ##$vtc= 25 ##$vtwait= 300 $$ sec ##$wbs= ##$werr= <> ##$wexp= ##$wnt= <> ##$wshim= ##$wtfile1= <> ##$wtfile= <> ##$x1= -86 ##$x2y2= 323 ##$x3= 119 ##$xy= 335 ##$xz2= 0 ##$xz= 65 ##$y1= 29 ##$y3= -138 ##$yz2= 0 ##$yz= -35 ##$z1= -108 ##$z1c= -56 ##$z2= -976 ##$z2c= 220 ##$z2x2y2= 0 ##$z2x3= 0 ##$z2xy= 0 ##$z2y3= 0 ##$z3= 62 ##$z3c= 0 ##$z3x2y2= 0 ##$z3x3= 0 ##$z3x= 0 ##$z3xy= 0 ##$z3y3= 0 ##$z3y= 0 ##$z4= -38 ##$z4c= 0 ##$z4x2y2= 0 ##$z4x= 0 ##$z4xy= 0 ##$z4y= 0 ##$z5= 0 ##$z5x= 0 ##$z5y= 0 ##$z6= 0 ##$z7= 0 ##$z8= 0 ##$zx2y2= 0 ##$zx3= 0 ##$zxy= 0 ##$zy3= 0 ##$rp= 55.0 ##$lp= -178.6 ##$rfl= 6632.3 ##$rfp= 5808.0 ##$axis=

##$sp= -75.9 ##$wp= 15236.6 ##$cr= 5808.0 ##$delta= 552.0 $$ End of Varian specific parameters $$ --------------------------------- $$ Y-values stored with standard (16-bit) integer precision ##DELTAX= -0.0066763383 ##XUNITS= PPM ##YUNITS= ARBITRARY UNITS $$ (mm on paper) ##XFACTOR= 1.0000000000 ##YFACTOR= 0.001553426 ##FIRSTX= 207.8365661484 ##LASTX= -10.9270117403 ##MAXY= 50.901126 ##MINY= -36.281829 ##NPOINTS= 32768 ##FIRSTY= 0.119614 ##XYDATA= (X++(Y..Y)) 207.83657G7J72R4o3j29o2J27J1j39n9j36j54NQ9q5L0J2q0J15k4j0P9O9K3l7M8n9p2J19r3q1n2r4 207.62292c59J46O6n8JL1j65Q7L3m6p4j22J74J73J00R1k03j33J96K26L0j4k77k6L25n5j09k3L5n 207.42931D5r2j77m5jN7J06Q4J67K14q0j23n4o6m0k3m9J01M9p9j39P5J12J36k8r2Q4K04Jk23j73 207.22902d9K7j4P9o8p6Q3P2J53k45j21O5L9J24K25J28k02l19j67J91J10o0j77M4L47J35j05k93K 207.04208g2m3j21M8J89J26n2p1j01Pj59m2P1J2O7K0N1J58j3nRJ91P3J3m7j60J2O2%k4M3qM2o7 206.82176B09j96m4k2j6j07J26R8J15R7j0jj03p3r6J1K42o6P0N3l22k75o4J29J42p3J5M6J05N9 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