##TITLE= NH 171; Ethyl 3-Chloropyrazine-2-carboxylate / CDCl3 ##JCAMP-DX= 5.00 $$ Varian Associates, Inc., VNMR Software $$ VNMR Version 5.1 Revision A, March 1, 1995 $$ Tue May 7 08:51:35 MET DST 2002 $$ svsj version 5.1, 97/1/14; hz2ppm (NH) ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= varian ##OWNER= N. Haider, University of Vienna ##SPECTROMETER/DATA SYSTEM= Varian UNITYplus-300 ##.OBSERVE FREQUENCY= 299.9484281 ##.OBSERVE NUCLEUS= ^1H ##.SOLVENT REFERENCE= 2.490 $$ solvent=cdcl3 ##.FIELD= 7.04 $$ Tesla ##.ACQUISITION TIME= 3.7376000 $$ seconds ##.AVERAGES= 16 $$ number of transients ##RESOLUTION= 0.153 $$ digital resolution in Hz ##.PHASE 0= -67.3 $$ zero order phase correction (left edge) ##.PHASE 1= 0.011201 $$ first order phase correction, deg/Hz ##$REFERENCE_POINT= 929.936 $$ Referencing label $$ Varian specific parameters $$ -------------------------- ##$acqstatus= (0..1) 17 1 ##$alfa= 19.9999923706 $$ usec ##$alock= ##$array= <> ##$arraydim= 1 ##$arrayelemts= 0 ##$at= 3.7376 ##$bs= 16 ##$celem= 1 ##$cp= ##$ct= 16 ##$d1= 2 $$ sec ##$d2= 0 $$ sec ##$date= ##$dfrq= 299.9479281 $$ Hz ##$dm= ##$dmf= 200 ##$dmm= ##$dn=

##$dod= 0.00999999977648 $$ sec ##$dof= 0 $$ Hz ##$dp= ##$dpwr= 30 ##$exppath= ##$fb= 2800 ##$file= ##$filter= 54.0999984741 ##$fn1= 1024 ##$gain= 40 ##$homo= ##$hs= ##$hst= 0.00800000037998 $$ sec ##$il= ##$in= ##$lb1= 0.318309992552 ##$load= ##$loc= 0 ##$math= ##$method= ##$np= 37376 ##$nt= 16 ##$p1= 0 $$ usec ##$pad= 0.5 $$ sec ##$parversion= 4.3 ##$pmode= ##$priority= 5 ##$proc1= ##$proc= ##$pslabel= ##$pw90= 16.8 $$ usec ##$pw= 10 $$ usec ##$rfband= ##$rof1= 10 $$ usec ##$rof2= 9.9999961853 $$ usec ##$seqfil= ##$sfrq= 299.9484281 ##$sn= 0 ##$solvent= ##$ss= 0 ##$sw= 5000 ##$temp= 28 ##$tin= ##$tn=

##$tof= 500 $$ Hz ##$tpwr= 57 ##$vtc= 25 ##$vtwait= 300 $$ sec ##$wbs= <> ##$werr= <> ##$wexp= <> ##$wnt= <> ##$wshim= ##$wtfile1= <> ##$wtfile= <> ##$x1= -86 ##$x2y2= 323 ##$x3= 119 ##$xy= 335 ##$xz2= 0 ##$xz= 65 ##$y1= 29 ##$y3= -138 ##$yz2= 0 ##$yz= -35 ##$z1= -108 ##$z1c= -56 ##$z2= -976 ##$z2c= 220 ##$z2x2y2= 0 ##$z2x3= 0 ##$z2xy= 0 ##$z2y3= 0 ##$z3= 62 ##$z3c= 0 ##$z3x2y2= 0 ##$z3x3= 0 ##$z3x= 0 ##$z3xy= 0 ##$z3y3= 0 ##$z3y= 0 ##$z4= -38 ##$z4c= 0 ##$z4x2y2= 0 ##$z4x= 0 ##$z4xy= 0 ##$z4y= 0 ##$z5= 0 ##$z5x= 0 ##$z5y= 0 ##$z6= 0 ##$z7= 0 ##$z8= 0 ##$zx2y2= 0 ##$zx3= 0 ##$zxy= 0 ##$zy3= 0 ##$rp= -11.2 ##$lp= -56.0 ##$rfl= 1676.8 ##$rfp= 746.9 ##$axis=

##$sp= -30.1 ##$wp= 3059.5 ##$cr= 2642.4 ##$delta= 152.0 $$ End of Varian specific parameters $$ --------------------------------- $$ Y-values stored with standard (16-bit) integer precision ##DELTAX= -0.0005087138 ##XUNITS= PPM ##YUNITS= ARBITRARY UNITS $$ (mm on paper) ##XFACTOR= 1.0000000000 ##YFACTOR= 0.002316263 ##FIRSTX= 13.5687039198 ##LASTX= -3.1003196312 ##MAXY= 75.896989 ##MINY= -0.006949 ##NPOINTS= 32768 ##FIRSTY= 0.016214 ##XYDATA= (X++(Y..Y)) 13.56870G%TjJjJjJ%Jj%VjKj%UJkJjJ%jKkJTj%VJlLkKkJ%TjJjJTjJjTJjJjJjJ%Jj%VjKj%jJjJ%U 13.52801GjJ%VJkJj%J%JkK%kJ%Jj%jJ%UjJ%jJjKkJ%TjJ%JkJ%UJj%jJ%ZjJ%TjJ%jJ%UJkJ%YjKkJ% 13.48324Gj%J%TjJjJkKjJ%TjKjTKk%UJj%Jj%J%jJ%j%JT%j%Vj%Jj%TJjJ%Yj%TJ%jJjJ%Tj%TJ%UJk 13.44203FJj%VJ%Uj%J%TJj%jTK%jJjkLj%J%TjJjJj%TJ%j%TJjJjJjJj%UJ%jJjJjJkKjJj%J%TjJjJ 13.40337Gj%JjJ%VjJ%UjJ%j%TJj%TJjJjJjJ%j%JjKlK%UjTKjJj%UJj%JjTJ%Jj%TJjJj%Jj%VJkJ%j 13.36318EKjTKj%TJjJj%KkJj%JjJ%j%jJT%Tj%jJTj%JjTJ%UJkKkJ%UjK%j%J%kJj%J%JjT%Kj%WJj% 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